1O1O
Deoxy hemoglobin (A,C:V1M,V62L; B,D:V1M,V67L)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1999-02-15 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.094, 83.218, 53.655 |
Unit cell angles | 90.00, 99.29, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.18 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1c7b |
RMSD bond length | 0.005 |
RMSD bond angle | 0.015 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.047 | 0.218 |
Number of reflections | 47581 | |
<I/σ(I)> | 14.9 | 4.85 |
Completeness [%] | 93.8 | 90.1 |
Redundancy | 2.81 | 2.76 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.50 |