Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-01-01 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 85.334, 93.070, 98.795 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.400 |
R-factor | 0.156 |
Rwork | 0.156 |
R-free | 0.16100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6xia |
RMSD bond length | 0.007 |
RMSD bond angle | 1.770 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.430 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.050 | |
Number of reflections | 154724 | |
<I/σ(I)> | 43.8 | 12.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 14.5 | 14.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | MPD, MgCl2, TRIS, pH 7.00 |