1NZJ
Crystal Structure and Activity Studies of Escherichia Coli Yadb ORF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-03-08 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 115.920, 39.300, 69.150 |
Unit cell angles | 90.00, 116.19, 90.00 |
Refinement procedure
Resolution | 24.254 - 1.500 |
R-factor | 0.14729 |
Rwork | 0.146 |
R-free | 0.16969 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gln |
RMSD bond length | 0.009 |
RMSD bond angle | 1.204 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 62.020 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.057 | 0.283 |
Number of reflections | 43648 | |
<I/σ(I)> | 9.1 | 2.5 |
Completeness [%] | 99.4 | 99.4 |
Redundancy | 3.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | PEG4000, MPD, Nacacodylate, pH 6.00, VAPOR DIFFUSION, SITTING DROP, temperature 293K |