1NPK
REFINED X-RAY STRUCTURE OF DICTYOSTELIUM NUCLEOSIDE DIPHOSPHATE KINASE AT 1,8 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 63 2 2 |
Unit cell lengths | 74.200, 74.200, 105.140 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.196 |
Rwork | 0.196 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.280 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 1.800 * | 1.800 * |
Rmerge | 0.067 * | 0.350 * |
Total number of observations | 57800 * | |
Number of reflections | 14427 * | |
Completeness [%] | 93.5 * | 84 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | 18 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PEG6000 | 5 (%) | |
2 | 1 | drop | 20 (mM) | ||
3 | 1 | drop | Tris-HCl | 50 (mM) | |
4 | 1 | reservoir | PEG6000 | 10 (%) | |
5 | 1 | reservoir | Tris-HCl | 50 (mM) |