Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1NPG

MYOGLOBIN (HORSE HEART) WILD-TYPE COMPLEXED WITH NITROSOETHANE

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2002-09-11
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameP 1 21 1
Unit cell lengths35.165, 28.706, 63.032
Unit cell angles90.00, 106.22, 90.00
Refinement procedure
Resolution40.000 - 1.700
R-factor0.2
Rwork0.200
R-free0.22700

*

Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1dwr
RMSD bond length0.005
RMSD bond angle1.414

*

Data reduction softwared*TREK
Data scaling softwared*TREK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0001.760
High resolution limit [Å]1.7001.700
Rmerge0.0380.201
Total number of observations39336

*

Number of reflections13504

*

1323

*

<I/σ(I)>24.45.1
Completeness [%]99.498.2
Redundancy2.892.76
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.4AMMONIUM SULFATE, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 100K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein30 (mg/ml)
21dropTris-HCl100 (mM)pH7.4
31dropammonium sulfate3.4-4.0 (M)
41dropTris-HCl100 (mM)pH7.4
51reservoirammonium sulfate3.1-3.3 (M)
61reservoirTris-HCl100 (mM)pH7.4

225158

PDB entries from 2024-09-18

PDB statisticsPDBj update infoContact PDBjnumon