1NOO
CYTOCHROME P450-CAM COMPLEXED WITH 5-EXO-HYDROXYCAMPHOR
Experimental procedure
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Collection date | 1994-10-25 |
Detector | SIEMENS-NICOLET X100 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 109.000, 104.300, 36.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.200 |
R-factor | 0.171 |
Rwork | 0.171 |
RMSD bond length | 0.007 |
RMSD bond angle | 22.960 * |
Data reduction software | XENGEN |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.098 |
Number of reflections | 20570 |
Completeness [%] | 94.0 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | free interface diffusion method * | 7 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | dithiothreitol | 50 (mM) |