1NLS

CONCANAVALIN A AND ITS BOUND SOLVENT AT 0.94A RESOLUTION

Experimental procedure

Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Temperature [K]	110
Detector technology	CCD
Collection date	1994
Spacegroup name	I 2 2 2
Unit cell lengths	89.550, 86.460, 62.110
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 0.940
R-factor	0.127
R-free	0.15400
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SHELXL-97
Refinement software	SHELXL-97

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]		1.010
High resolution limit [Å]		0.940
Rmerge	0.093	0.150
Number of reflections	116923
Completeness [%]	75.4	30.4
Redundancy	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.8		pH 6.8