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1NIV

MANNOSE-SPECIFIC AGGLUTININ (LECTIN) FROM SNOWDROP (GALANTHUS NIVALIS) BULBS IN COMPLEX WITH MANNOSE-ALPHA 1,3-METHYL-D-MANNOSE

Experimental procedure
Detector technologyIMAGE PLATE
Collection date1994-09-09
DetectorRIGAKU
Spacegroup nameI 21 3
Unit cell lengths138.149, 138.149, 138.149
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution8.000 - 3.000
R-factor0.226

*

Rwork0.227
R-free0.26900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)GNA-ALPHA-MEMAN COMPLEX
RMSD bond length0.008
RMSD bond angle1.500

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]3.110
High resolution limit [Å]3.0003.000
Rmerge0.1070.289
Total number of observations39125

*

Number of reflections8280
<I/σ(I)>92.9
Completeness [%]93.186.3
Redundancy4.72.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

8.5

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein25 (mg/ml)
211ammonium bicarbonate0.05 (M)
311MeMan-20.023 (M)

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