1NDQ
Bacillus lentus subtilisin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.600, 62.400, 75.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
R-factor | 0.174 |
Rwork | 0.174 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Phasing software | CNX |
Refinement software | CNX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 2.000 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.068 | |
Number of reflections | 18308 | |
Completeness [%] | 85.0 | 75 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |