1NC7
Crystal Structure of Thermotoga maritima 1070
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-08-29 |
| Detector | SBC-2 |
| Wavelength(s) | 0.97932, 0.97952, 0.946 |
| Spacegroup name | P 1 |
| Unit cell lengths | 54.435, 54.453, 55.178 |
| Unit cell angles | 63.18, 62.27, 89.81 |
Refinement procedure
| Resolution | 29.400 - 1.550 |
| R-factor | 0.171 |
| Rwork | 0.170 |
| R-free | 0.19000 |
| Structure solution method | MAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.300 |
| Data reduction software | HKL-2000 |
| Data scaling software | d*TREK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.400 | 1.610 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Rmerge | 0.055 | |
| Number of reflections | 66002 | |
| <I/σ(I)> | 8.5 | |
| Completeness [%] | 94.3 | 74.3 |
| Redundancy | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | Sodium Formate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
