1NA1

The structure of HRV14 when complexed with Pleconaril

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (3.3 Å)

Cell axes437.160437.160437.160
Cell angles90.0090.0090.00
SpacegroupP 21 3
Resolution limits20.00 - 3.30
the highest resolution shell value -
R-factor0.223
R-work0.22200
R-free0.22800
RMSD bond length0.010*
RMSD bond angle1.540*

Data Collection Statistics

Resolution limits20.00 - 3.30
the highest resolution shell value -
Number of reflections320952
Number of measurements545390*
Rmerge_l_obs0.164*
the highest resolution shell value0.477*
Completeness77.8
the highest resolution shell value68.2*
I/sigma(I)0

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP7.5293unknown*

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirHEPES0.25 (M)
21reservoir0.25 (M)
31reservoir0.1 (M)
41reservoirPEG80000.3 (%)
51dropprotein20000 (mg/ml)
Annotated Information is extracted from Literature Info*