1N68
Copper bound to the Multicopper Oxidase CueO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-05-16 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.378 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.000, 90.941, 53.809 |
Unit cell angles | 90.00, 102.35, 90.00 |
Refinement procedure
Resolution | 26.300 - 1.700 |
R-factor | 0.171 |
Rwork | 0.165 |
R-free | 0.22200 |
Starting model (for MR) | 1kv7 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.024 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.300 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 51492 | |
<I/σ(I)> | 11.6 | 3 |
Completeness [%] | 99.7 | 100 |
Redundancy | 4.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 295 | 20% PEG, 200 MM AMMONIUM ACETATE, 100 MM SODIUM ACETATE,10 MM COPPER CHLORIDE , pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 295K |