1N00
Annexin Gh1 from cotton
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X9B |
Synchrotron site | NSLS |
Beamline | X9B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-06-24 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97950 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 61.049, 61.049, 215.355 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.720 - 2.100 |
R-factor | 0.219 |
Rwork | 0.219 |
R-free | 0.28000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 20.900 * |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.230 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.043 * | 0.433 * |
Total number of observations | 808320 * | |
Number of reflections | 27412 | |
Completeness [%] | 100.0 | 100 * |
Redundancy | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 * | 285 | ammonium sulfate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 285K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | 0-1 (M) | ||
2 | 1 | drop | HEPES | 20 (%saturated) | pH8.0 |
3 | 1 | drop | 230-350 (mM) | ||
4 | 1 | reservoir | ammonium sulfate | 1.7 (M) | |
5 | 1 | reservoir | HEPES | 0.1 (M) | pH7.0 |