1MZM

MAIZE NONSPECIFIC LIPID TRANSFER PROTEIN COMPLEXED WITH PALMITATE

Experimental procedure

Detector technology	AREA DETECTOR
Spacegroup name	P 21 21 21
Unit cell lengths	24.800, 49.600, 70.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.780
R-factor	0.171
Rwork	0.171
R-free	0.17900
RMSD bond length	0.013
RMSD bond angle	1.720
Data reduction software	MADNES
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.038
Total number of observations	22364 *
Number of reflections	7449
Completeness [%]	84.9
Redundancy	4.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		24.5-25.5 *	Shin, D.H., (1994) Proteins: Struct.,Funct., Genet., 19, 80. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1		24-well tissue culture plates		flow laboratories