1MYK
CRYSTAL STRUCTURE, FOLDING, AND OPERATOR BINDING OF THE HYPERSTABLE ARC REPRESSOR MUTANT PL8
Experimental procedure
Spacegroup name | P 41 21 2 |
Unit cell lengths | 51.800, 51.800, 110.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.400 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.27700 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.490 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 6.000 * | |
High resolution limit [Å] | 2.400 * | 2.400 * |
Rmerge | 0.094 * | |
Number of reflections | 5340 | |
Completeness [%] | 90.4 | 56.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | drop | bis-tris propane-HCl | 30 (mM) | |
3 | 1 | drop | 1 (mM) | ||
4 | 1 | drop | PEG3400 | 22-24 (%) | precipitant |
5 | 1 | drop | 2-propanol | 7-9 (%) | precipitant |
6 | 1 | drop | NaHEPES | 100 (mM) | precipitant |
7 | 1 | reservoir | precipitant |