1MUP
PHEROMONE BINDING TO TWO RODENT URINARY PROTEINS REVEALED BY X-RAY CRYSTALLOGRAPHY
Experimental procedure
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 57.300, 57.300, 110.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 14.000 - 2.400 |
| R-factor | 0.191 |
| Rwork | 0.191 |
| RMSD bond length | 0.026 |
| RMSD bond angle | 0.080 * |
| Phasing software | X-PLOR |
| Refinement software | PROLSQ |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 5.5 * | taken from Bocskei, Z. et al (1991). J. Mol. Biol., 218, 699-701. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 12 (mg/ml) | |
| 2 | 1 | drop | maleate | 30 (mM) | |
| 3 | 1 | drop | 0.005ml of well solution | ||
| 4 | 1 | reservoir | 40-70 (mM) | ||
| 5 | 1 | reservoir | maleate | 200 (mM) |
