1MTW
FACTOR XA SPECIFIC INHIBITOR IN COMPLEX WITH BOVINE TRYPSIN
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 287 |
Detector technology | AREA DETECTOR |
Collection date | 1994-11 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.900, 61.000, 64.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.900 |
R-factor | 0.169 |
Rwork | 0.169 |
Structure solution method | DIFFERENCE FOURIER |
RMSD bond length | 0.009 |
RMSD bond angle | 24.700 * |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.032 | 0.119 |
Total number of observations | 25539 * | |
Number of reflections | 16195 | |
<I/σ(I)> | 12 | 3 |
Completeness [%] | 91.7 | 80.3 |
Redundancy | 1.6 | 1.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8 | 0.3M AMMONIUM SULFATE, PH 8.0, 30% PEG 8000 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 0.3 (M) | |
2 | 1 | reservoir | PEG8000 | 30 (%) |