1MSB
STRUCTURE OF THE CALCIUM-DEPENDENT LECTIN DOMAIN FROM A RAT MANNOSE-BINDING PROTEIN DETERMINED BY MAD PHASING
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.400, 73.100, 45.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.300 |
Rwork | 0.176 |
RMSD bond length | 0.010 |
RMSD bond angle | 2.600 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Rmerge | 0.031 * |
Number of reflections | 7195 * |
Completeness [%] | 89.3 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 20 (mg/ml) | |
2 | 1 | drop | 10 (mM) | ||
3 | 1 | drop | 5 (mM) | ||
4 | 1 | drop | 1.1 (mM) | ||
5 | 1 | reservoir | PEG3350 | 15-20 (%) | or PEG8000 |
6 | 1 | reservoir | 20 (mM) | ||
7 | 1 | reservoir | Tris-HCl | 100 (mM) | |
8 | 1 | reservoir | 10 (mM) | ||
9 | 1 | reservoir | 0.02 (%) |