1MSA
MANNOSE-SPECIFIC AGGLUTININ (LECTIN) FROM SNOWDROP (GALANTHUS NIVALIS) BULBS COMPLEXED WITH METHYL-ALPHA-D-MANNOSIDE
Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1993-02-20 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 138.820, 64.110, 62.080 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.295 * |
| R-factor | 0.177 |
| Rwork | 0.177 |
| R-free | 0.24000 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 27.240 * |
| Data reduction software | SOFTWARE (PROVIDED BY MAXD) |
| Phasing software | X-PLOR (3.0) |
| Refinement software | X-PLOR (3.0) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.295 * |
| Rmerge | 0.044 |
| Number of reflections | 23359 |
| Completeness [%] | 91.7 |
| Redundancy | 3.49 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 8 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ammonium sulfate | 45 (%) | |
| 2 | 1 | 1 | Me-alpha-Man | 0.5-1.0 (M) |
