1MMR
MATRILYSIN COMPLEXED WITH SULFODIIMINE INHIBITOR
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1994-03-22 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 62.100, 62.100, 87.400 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 6.000 - 2.400 |
| R-factor | 0.187 |
| Rwork | 0.187 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 2.880 |
| Data reduction software | MOSFLM (V. 5.1.2) |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.300 * |
| Rmerge | 0.080 |
| Total number of observations | 23346 * |
| Number of reflections | 7690 |
| Completeness [%] | 95.5 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 17-25 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 10 (mg/ml) | |
| 2 | 1 | drop | inhibitor | 1.2 (mM) | |
| 3 | 1 | drop | DMSO | 2.5 (%) | |
| 4 | 1 | reservoir | 1.5 (M) | ||
| 5 | 1 | reservoir | ethanol | 10 (%) |
