1MJY

STRUCTURE OF INORGANIC PYROPHOSPHATASE MUTANT D70N

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1996-04
Detector	MARRESEARCH
Spacegroup name	H 3 2
Unit cell lengths	104.483, 104.483, 172.953
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	15.000 - 2.100
Rwork	0.164
R-free	0.23100
RMSD bond length	0.015
RMSD bond angle	0.037
Refinement software	REFMAC

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.085
Number of reflections	21273
Completeness [%]	99.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	potassium phosphate	0.1 (M)
2	1	1	PEG2000	1 (%)
3	1	2	ammonium chloride