1MJV
DISULFIDE DEFICIENT MUTANT OF VASCULAR ENDOTHELIAL GROWTH FACTOR A (C51A and C60A)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2000-06-25 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 29.280, 77.200, 55.110 |
Unit cell angles | 90.00, 98.92, 90.00 |
Refinement procedure
Resolution | 19.000 - 2.100 |
R-factor | 0.203 |
Rwork | 0.196 |
R-free | 0.24800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vpf |
RMSD bond length | 0.100 |
RMSD bond angle | 1.500 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.000 | 2.200 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.068 | 0.274 |
Number of reflections | 14119 | |
<I/σ(I)> | 12.5 | 4.3 |
Completeness [%] | 99.5 | 99.9 |
Redundancy | 3.4 | 3.36 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | Na-Citrate, isopropanol, PEG4000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |