Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-D |
Synchrotron site | APS |
Beamline | 14-BM-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-03-20 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 55.130, 55.130, 80.142 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.050 - 1.700 |
R-factor | 0.176 |
Rwork | 0.164 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.440 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.050 | 1.740 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 13471 | |
Completeness [%] | 83.1 | 23.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 1.8 mM ammonium sulfate, 50 mM MES (pH 6.5), and 5% dioxane, pH 6.50, VAPOR DIFFUSION, HANGING DROP, temperature 298K |