1MBB

OXIDOREDUCTASE

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	50.000, 50.000, 264.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	12.000 - 2.300
R-factor	0.238
Rwork	0.238
R-free	0.32400
RMSD bond length	0.012
RMSD bond angle	2.680
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	12.000
High resolution limit [Å]	2.300
Rmerge	0.072 *
Total number of observations	52502 *
Number of reflections	14935
Completeness [%]	94.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8 *	25 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	enzyme	5.7 (mM)
2	1	reservoir	PEG8000	13-14 (%)
3	1	reservoir	HEPES	100 (mM)
4	1	reservoir	calcium acetate	200 (mM)