1MAZ
X-RAY STRUCTURE OF BCL-XL, AN INHIBITOR OF PROGRAMMED CELL DEATH
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-11-01 |
Detector | RIGAKU |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 63.500, 63.500, 110.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.200 |
R-factor | 0.192 |
Rwork | 0.192 |
R-free | 0.25900 |
RMSD bond length | 0.014 * |
RMSD bond angle | 1.920 * |
Data reduction software | HKL |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.055 |
Number of reflections | 11139 |
Completeness [%] | 94.0 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 25 (mg/ml) | |
2 | 1 | drop | Tris | 50 (mM) | |
3 | 1 | reservoir | PEG4000 | 28-31 (%(w/v)) | |
4 | 1 | reservoir | ammonium acetate | 0.2 (M) | |
5 | 1 | reservoir | sodium citrate | 0.1 (M) |