1MAM
CRYSTAL STRUCTURE TO 2.45 A RESOLUTION OF A MONOCLONAL FAB SPECIFIC FOR THE BRUCELLA A CELL WALL POLYSACCHARIDE ANTIGEN
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.730, 126.820, 46.820 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.450 |
R-factor | 0.215 |
RMSD bond length | 0.013 |
RMSD bond angle | 0.034 * |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.420 * |
Rmerge | 0.052 * |
Total number of observations | 37288 * |
Number of reflections | 15355 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Fab | 0.004 ml | |
2 | 1 | drop | ammonium sulfate | 0.12 (M) | 0.001 ml |
3 | 1 | drop | Tris-HCl | 0.5 (M) | 0.0008 ml |
4 | 1 | drop | PEG8000 | 20 (%(w/v)) | 0.0042 ml |
5 | 1 | reservoir | PEG8000 | 34 (%) | 0.001 ml |
6 | 1 | reservoir | sodium azide | trace amount |