Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 93 |
| Detector technology | IMAGE PLATE |
| Collection date | 2000-12-22 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 142.880, 142.880, 111.310 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 71.440 - 1.900 |
| R-factor | 0.198 |
| Rwork | 0.194 |
| R-free | 0.24200 |
| Structure solution method | MIR |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.300 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MLPHARE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 1.850 | 1.920 |
| High resolution limit [Å] | 1.400 | 1.850 |
| Number of reflections | 34328 | |
| <I/σ(I)> | 21.2 | 3.2 |
| Completeness [%] | 99.6 | 98.7 |
| Redundancy | 5.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 278 | PEG 6000, LITHIUM SULPHATE, SODIUM CITRATE, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 278K |
