1M70
Crystal structure of oxidized recombinant cytochrome c4 from Pseudomonas stutzeri
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2000-12-07 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54179 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.960, 57.640, 84.410 |
Unit cell angles | 90.00, 104.23, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.250 |
R-factor | 0.1571 |
Rwork | 0.155 |
R-free | 0.20210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1etp |
RMSD bond length | 0.011 |
RMSD bond angle | 0.028 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.290 |
High resolution limit [Å] | 1.250 | 1.250 |
Number of reflections | 175219 | |
Completeness [%] | 90.9 | 77 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 298 | 0.2M ammonium acetate, 0.1M sodium citrate pH 5.6, 30%(w/v) PEG 4000, pH 6.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 298 | 0.2M ammonium acetate, 0.1M sodium citrate pH 5.6, 30%(w/v) PEG 4000, pH 6.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |