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1M6Z

Crystal structure of reduced recombinant cytochrome c4 from Pseudomonas stutzeri

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsMAX II BEAMLINE I711
Synchrotron siteMAX II
BeamlineI711
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2001-01-26
DetectorMARRESEARCH
Wavelength(s)1.03260
Spacegroup nameP 1 21 1
Unit cell lengths75.110, 57.560, 83.750
Unit cell angles90.00, 104.32, 90.00
Refinement procedure
Resolution30.000 - 1.350
R-factor0.1427
Rwork0.140
R-free0.19070
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1etp
RMSD bond length0.010
RMSD bond angle0.028
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.400
High resolution limit [Å]1.3501.350
Number of reflections142653
Completeness [%]93.587
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.62980.2M ammonium acetate, 0.1M sodium citrate pH 5.6, 30%(w/v) PEG 4000, 5%(v/v) glycerol, pH 6.6, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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