1M45
CRYSTAL STRUCTURE OF MLC1P BOUND TO IQ2 OF MYO2P, A CLASS V MYOSIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-D |
Synchrotron site | APS |
Beamline | 14-BM-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-06-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.594, 56.455, 56.928 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.650 |
R-factor | 0.19284 |
Rwork | 0.191 |
R-free | 0.22788 |
Structure solution method | MOLECULAR REPLACEMENT, Structure of MLC1P bound to IQ 2 AND 3 (SOLVED BY MAD METHOD) |
RMSD bond length | 0.013 |
RMSD bond angle | 1.365 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.400 | 1.710 |
High resolution limit [Å] | 1.640 | 1.640 |
Rmerge | 0.036 | 0.200 |
Number of reflections | 17258 | |
<I/σ(I)> | 25.6 | 6.1 |
Completeness [%] | 97.1 | 86 |
Redundancy | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, sodium chloride, VAPOR DIFFUSION, HANGING DROP, temperature 293K |