1LZ4

ENTHALPIC DESTABILIZATION OF A MUTANT HUMAN LYSOZYME LACKING A DISULFIDE BRIDGE BETWEEN CYSTEINE-77 AND CYSTEINE-95

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	56.820, 60.860, 33.330
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	5.000 - 1.800
R-factor	0.188
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.760 *
Rmerge	0.056 *
Total number of observations	40579 *
Number of reflections	11258 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6 *	13.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	20 (mg/ml)
2	1	reservoir		2.5 (M)
3	1	reservoir	sodium phosphate	30 (mM)