1LUR
Crystal Structure of the GalM/aldose Epimerase Homologue from C. elegans, Northeast Structural Genomics Target WR66
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2001-08-15 |
| Detector | RIGAKU RAXIS |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 50.808, 91.007, 83.701 |
| Unit cell angles | 90.00, 100.67, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.850 |
| R-factor | 0.224 |
| Rwork | 0.224 |
| R-free | 0.26200 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.509 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS (1.1) |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 100.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 131853 |
| <I/σ(I)> | 24.35 |
| Completeness [%] | 92.9 |
| Redundancy | 3.36 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.2 | 294 | PEG 600, Lithium Sulfate, TrisCl, PEG 4000, Glycerol, pH 8.2, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
