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1LU5

2.4 Angstrom Crystal Structure of the Asymmetric Platinum Complex {Pt(ammine)(cyclohexylamine)}2+ Bound to a Dodecamer DNA Duplex

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2001-08-12
DetectorMARRESEARCH
Wavelength(s)0.97
Spacegroup nameP 1
格子定数 [Å]31.644, 35.638, 46.556
格子定数 [度]79.53, 83.02, 81.36
精密化法
残基50.000 - 2.400
R-free0.24950

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Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1aio
結合長の平均二乗偏差(RMSD) [Å]0.005
結合角の平均二乗偏差(RMSD) [度]0.022
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSHELXS
Refinement softwareSHELXL-97
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)50.0002.490
分解能 [Å] (高)2.4002.400
Rmerge_l_obs0.090

*

0.277

*

Total number of observations42245

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独立反射数7337
<I/σ(I)>9.2
完全性 [%]96.396.3
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP6.54.

*

spermine, sodium cacodylate, magnesium acetate, PEG 4000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K
結晶化試薬
ID結晶ID濃度試薬名濃度 (単位)詳細
111spermine
211sodium cacodylate
311magnesium acetate
411PEG 4000
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropprotein0.2 (mM)
21reservoir50 (mM)pH6.5
31reservoirspermine12 (mM)
41reservoir120 (mM)
51reservoirPEG400015 (%(w/v))

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件を2024-09-18に公開中

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