1LTW
RECOMBINANT SPERM WHALE MYOGLOBIN 29W MUTANT (OXY)
Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 6 |
Unit cell lengths | 91.461, 91.461, 45.841 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 5.000 - 1.700 |
R-factor | 0.158 |
Rwork | 0.158 |
RMSD bond length | 0.018 |
RMSD bond angle | 20.560 * |
Data reduction software | RIGAKU |
Data scaling software | RIGAKU |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.600 |
Rmerge | 0.087 |
Number of reflections | 17658 |
Completeness [%] | 71.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.4 * | pH 9 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium salfate | 2.2-2.6 (M) | |
2 | 1 | 1 | Tris-HCl | 20 (mM) | |
3 | 1 | 1 | EDTA | 1 (mM) | |
4 | 1 | 2 | sodium phosphate | 50 (mM) | pH7.4 |