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1LR6

Crystal structure of V45Y mutant of cytochrome b5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSEALED TUBE
Temperature [K]293
Detector technologyIMAGE PLATE
Collection date1999-11-10
DetectorMARRESEARCH
Wavelength(s)1.5418
Spacegroup nameC 1 2 1
Unit cell lengths69.404, 40.441, 39.196
Unit cell angles90.00, 111.70, 90.00
Refinement procedure
Resolution22.820 - 1.900
R-factor0.191
Rwork0.191
R-free0.23500

*

Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)1ehb
RMSD bond length0.008
RMSD bond angle1.165

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]22.8201.940
High resolution limit [Å]1.9001.900
Rmerge0.0620.194
Number of reflections7563
<I/σ(I)>6.1
Completeness [%]93.576.3
Redundancy3.12.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5293PHOSPHATE BUFFER, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein20 (mg/ml)
21reservoirphosphate3.1 (M)pH7.5

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