1LPM
A STRUCTURAL BASIS FOR THE CHIRAL PREFERENCES OF LIPASES
Experimental procedure
Spacegroup name | C 2 2 21 |
Unit cell lengths | 65.200, 97.500, 176.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.200 * |
R-factor | 0.139 |
Rwork | 0.139 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.820 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 * |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.107 * |
Total number of observations | 68189 * |
Number of reflections | 25316 |
Completeness [%] | 84.8 |
Redundancy | 2.7 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 5.3 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 8 (mg/ml) | |
2 | 1 | reservoir | MPD | 40 (%(v/v)) | |
3 | 1 | reservoir | sodium acetate | 30 (mM) | |
4 | 1 | reservoir | 30 (mM) |