1LJH
CRYSTAL STRUCTURE OF MONOCLINIC LYSOZYME GROWN IN PRESENCE OF 5% GLYCEROL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 27.909, 62.808, 60.331 |
Unit cell angles | 90.00, 90.56, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.800 |
R-factor | 0.198 |
Rwork | 0.198 |
R-free | 0.22600 |
RMSD bond length | 0.005 |
RMSD bond angle | 23.300 * |
Data scaling software | SCALEPACK |
Refinement software | CNS (0.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.046 * | 0.139 * |
Total number of observations | 114902 * | |
Number of reflections | 18861 * | 1862 * |
Completeness [%] | 97.2 * | 95.1 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.6 | 293 | Sodium Acetate(0.1M)-Buffer, Sodium Nitrate (0.44M)-Precipitant, glycerol(0.54M) - Additive, pH 4.6, LIQUID DIFFUSION at 293K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | sodium acetate | 0.1 (M) | pH4.6 |
2 | 1 | 1 | glycerol | 5 (%) |