1LJ3
CRYSTAL STRUCTURE OF MONOCLINIC LYSOZYME GROWN AT PH 4.6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 27.886, 62.760, 60.273 |
Unit cell angles | 90.00, 90.91, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.178 |
Rwork | 0.178 |
R-free | 0.23300 |
RMSD bond length | 0.005 |
RMSD bond angle | 23.200 * |
Data reduction software | AUTOMAR |
Refinement software | CNS (0.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.052 * | 0.161 * |
Total number of observations | 39179 * | |
Number of reflections | 13653 * | 1311 * |
Completeness [%] | 96.7 * | 95.7 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.6 | 293 * | Sodium Acetate (0.1M) Buffer, Sodium Nitrate (0.44M) Precipitant, pH 4.6, LIQUID DIFFUSION at 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | sodium acetate | 0.1 (M) | pH4.6 |