Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-11-10 |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.100, 68.000, 56.800 |
| Unit cell angles | 90.00, 100.80, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.500 |
| R-factor | 0.2 |
| Rwork | 0.198 |
| R-free | 0.26000 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.903 |
| Data reduction software | bioteX |
| Data scaling software | bioteX |
| Phasing software | MERLOT |
| Refinement software | TNT |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 10.000 | 2.700 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.099 | 0.230 |
| Number of reflections | 28789 | |
| <I/σ(I)> | 10 | |
| Completeness [%] | 95.0 | 85 |
| Redundancy | 2 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.50 |
