1LIC

X-RAY CRYSTALLOGRAPHIC STRUCTURES OF ADIPOCYTE LIPID BINDING PROTEIN COMPLEXED WITH PALMITATE AND HEXADECANESULFONIC ACID. PROPERTIES OF CAVITY BINDING SITES.

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	120.800, 37.760, 28.600
Unit cell angles	90.00, 92.20, 90.00

Refinement procedure

Resolution	10.000 - 1.600
R-factor	0.195
Rwork	0.195
R-free	0.22500
RMSD bond length	0.021
RMSD bond angle	1.470
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.600 *
Rmerge	0.029 *
Total number of observations	63130 *
Number of reflections	17182 *
Completeness [%]	96.0 *
Redundancy	4.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1		2.1-3.0 (M)