1LHZ
Structure of a Human Bence-Jones Dimer Crystallized in U.S. Space Shuttle Mission STS-95: 293K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1998-11-19 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.940, 85.170, 114.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.300 |
Rwork | 0.173 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jvk |
RMSD bond length | 0.130 |
RMSD bond angle | 1.780 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.077 | 0.161 * |
Total number of observations | 92994 * | |
Number of reflections | 21254 * | 1943 * |
<I/σ(I)> | 16.1 | 7.6 |
Completeness [%] | 98.3 | 91.7 |
Redundancy | 4.4 | 3.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 279 | Alvarado, U.R., (2001) J. Crystal Growth, 223, 407. * |