1LHS
LOGGERHEAD SEA TURTLE MYOGLOBIN (AQUO-MET)
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-10-02 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.500, 61.100, 75.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.000 |
R-factor | 0.182 |
RMSD bond length | 0.018 * |
RMSD bond angle | 2.650 * |
Data reduction software | MOSFLM |
Phasing software | X-PLOR (3.1) |
Refinement software | TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 * |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.036 * |
Total number of observations | 58570 * |
Number of reflections | 13820 |
Completeness [%] | 97.7 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 25 (mg/ml) | |
2 | 1 | 2 | ammonium sulfate | 3.2 (M) | |
3 | 1 | 2 | Tris-HCl | 0.05 (M) |