1LHS

LOGGERHEAD SEA TURTLE MYOGLOBIN (AQUO-MET)

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1994-10-02
Detector	RIGAKU
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	37.500, 61.100, 75.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 2.000
R-factor	0.182
RMSD bond length	0.018 *
RMSD bond angle	2.650 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	15.000 *
High resolution limit [Å]	2.000 *
Rmerge	0.036 *
Total number of observations	58570 *
Number of reflections	13820
Completeness [%]	97.7
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	25 (mg/ml)
2	1	2	ammonium sulfate	3.2 (M)
3	1	2	Tris-HCl	0.05 (M)