1LEN

REFINEMENT OF TWO CRYSTAL FORMS OF LENTIL LECTIN AT 1.8 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	58.490, 56.370, 82.730
Unit cell angles	90.00, 104.40, 90.00

Refinement procedure

Resolution	? - 1.800
R-factor	0.175
RMSD bond length	0.017 *
RMSD bond angle	0.037 *
Refinement software	RESTRAIN

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.750 *
Rmerge	0.065 *	0.269 *
Total number of observations	169906 *
Number of reflections	53882 *
Completeness [%]	83.7 *	74.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *	6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	3 (mg/ml)
2	1	1	phosphate	20 (mM)
3	1	1	acetate	20 (mM)	pH6.0
4	1	1	MPD	35-40 (%(v/v))