1LEK
Crystal Structure of H-2Kbm3 bound to dEV8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 170 |
Detector technology | AREA DETECTOR |
Collection date | 1997-12-13 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 135.894, 87.123, 45.231 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.150 |
Rwork | 0.206 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.720 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 2.230 |
High resolution limit [Å] | 2.150 | 2.150 |
Number of reflections | 29655 | |
Completeness [%] | 98.6 | 99.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.8 | 298 | sodium potassium phosphate, pH 6.8, VAPOR DIFFUSION, temperature 298K |