1LDC

X-RAY STRUCTURE OF TWO COMPLEXES OF THE Y143F FLAVOCYTOCHROME B2 MUTANT CRYSTALLIZED IN THE PRESENCE OF LACTATE OR PHENYL-LACTATE

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.9 Å)

Cell axes164.500164.500114.000
Cell angles90.0090.00120.00
SpacegroupP 32 2 1
Resolution limits6.00 - 2.90
the highest resolution shell value -
R-factor0.195
R-work0.19500
RMSD bond length0.010
RMSD bond angle3.700

Data Collection Statistics

Resolution limits100.00* - 2.90*
the highest resolution shell value -
Number of reflections30412
Number of measurements156473*
Rmerge_l_obs0.150
Completeness80.0
Redundancy7.4
I/sigma(I)1

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1Vapor diffusion*5.5*20**

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirPEG400010-12 (%(w/w))
21reservoirMES50 (mM)
Annotated Information is extracted from Literature Info*