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1L4B

Crystal Structure of CobT in apo state

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]278
Detector technologyAREA DETECTOR
DetectorSIEMENS HI-STAR
Wavelength(s)1.5418
Spacegroup nameP 21 21 2
Unit cell lengths72.100, 90.200, 47.500
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution500.000 - 1.700
Rwork0.191
R-free0.21800
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)1d0s
RMSD bond length0.009
RMSD bond angle1.340
Data reduction softwareXDS
Data scaling softwareXDS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]1.750
High resolution limit [Å]1.7001.700
Rmerge0.0630.279
Number of reflections31865
<I/σ(I)>13.81.6
Completeness [%]88.460.6
Redundancy3.31.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6298ammonium phosphate, pH 6.0, VAPOR DIFFUSION, HANGING DROP at 298K

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PDB entries from 2024-11-13

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