1L2P
ATP Synthase b Subunit Dimerization Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-08-20 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.99203 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 35.700, 40.760, 42.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.400 * - 1.550 |
R-factor | 0.282 * |
Rwork | 0.282 |
R-free | 0.31300 |
Structure solution method | MIR |
RMSD bond length | 0.005 |
RMSD bond angle | 13.100 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.610 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.027 | 0.117 |
Number of reflections | 9455 * | |
<I/σ(I)> | 25.1 | |
Completeness [%] | 93.5 * | 83.1 * |
Redundancy | 5.4 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291 | 30% ISOPROPANOL, 45% 2-METHYL-2,4-PENTANEDIOL, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 18.0K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 25 (mg/ml) | |
2 | 1 | reservoir | 2-propanol | 45 (%) | |
3 | 1 | reservoir | MPD | 30 (%) |