1KVS
UDP-GALACTOSE 4-EPIMERASE COMPLEXED WITH UDP-PHENOL
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 87 |
Detector technology | AREA DETECTOR |
Detector | SIEMENS HI-STAR |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 83.500, 83.500, 108.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.150 |
R-factor | 0.188 * |
Rwork | 0.188 |
RMSD bond length | 0.015 |
RMSD bond angle | 16.200 * |
Data scaling software | XSCALIBRE |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 2.150 | 2.150 * |
Rmerge | 0.064 | 0.245 * |
Total number of observations | 68358 * | |
Number of reflections | 24177 | 3002 * |
Completeness [%] | 95.0 | 87 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 9 | 4 * | pH 9.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 14-20 (%) | |
2 | 1 | reservoir | 500-750 (mM) | ||
3 | 1 | reservoir | CHES | 50 (mM) |