1KU0
Structure of the Bacillus stearothermophilus L1 lipase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 119.620, 85.040, 98.360 |
| Unit cell angles | 90.00, 99.73, 90.00 |
Refinement procedure
| Resolution | 99.000 - 2.000 |
| Rwork | 0.185 |
| R-free | 0.21800 |
| Structure solution method | MIR |
| Phasing software | SHARP |
| Refinement software | CNS (0.9) |
Data quality characteristics
| Overall | Outer shell | |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.059 | 0.222 |
| <I/σ(I)> | 20.2 | 6.1 |
| Completeness [%] | 96.9 | 95.2 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
