1KSO
CRYSTAL STRUCTURE OF APO S100A3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-03-20 |
Detector | MARRESEARCH |
Wavelength(s) | 0.934 |
Spacegroup name | P 31 |
Unit cell lengths | 58.769, 58.769, 45.338 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 * - 1.700 |
R-factor | 0.194 |
Rwork | 0.194 |
R-free | 0.22500 |
Structure solution method | MIR |
RMSD bond length | 0.005 |
RMSD bond angle | 18.200 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.810 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.038 * | 0.300 * |
Total number of observations | 34465 * | |
Number of reflections | 19298 * | |
Completeness [%] | 98.2 | 100 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.3 | 293 | tris, ammonium sulfate, pH 8.3, VAPOR DIFFUSION, SITTING DROP, temperature 20K |
1 | VAPOR DIFFUSION, SITTING DROP | 8.3 | 293 | tris, ammonium sulfate, pH 8.3, VAPOR DIFFUSION, SITTING DROP, temperature 20K |